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鉄と鋼
Vol. 66 (1980), No. 10

鉄と鋼 Vol. 66 (1980), No. 10

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オンライン版ISSN:	1883-2954
冊子版ISSN:	0021-1575
発行機関:	The Iron and Steel Institute of Japan

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キーワードランキング

21 Dec. (Last 30 Days)

鉄と鋼 Vol. 66 (1980), No. 10

Oxidation of Sulfur in B. F. Slags to Sulfate

Kimihisa ITO, Hitoshi MORISHITA, Nobuo SANO, Gaku WATANABE, Yukio MATSUSHITA

pp. 1459-1467

抄録

In order to remove the deteriorating effects of B. F. slag caused by the presence of sulfide, an investigation has been made of the oxidation of sulfide in B. F. slags to sulfate for samples in the form of planes or fluidized powders at 870 to 1200 °C.
The results obtained are as follows:
1) The optimum temperature to oxidize the sulfide to sulfate with suppressing the evolution of SO₂ is 1100 to 1200 °C for slag planes, and is 900 °C for slag powders, the difference between the two being due to the sintering during the oxidation for the latter.
2) The rate of oxidation of sulfide to sulfate is controlled by the diffusion of oxygen in the slag.
3) The dissolution of S= into water from treated B. F. slags can be prevented when more than 90% of sulfur exists as sulfate.
4) To achieve the result indicated in 3), it is estimated that slag powders of-200 mesh should be treated in the air for 2 hours at 870 °C, for example.

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Removal of Tellurium out of Molten Iron

Yoshimoto WANIBE, Kohji SAWADA, Toshiharu FUJISAWA, Hiroshi SAKAO

pp. 1468-1473

抄録

The co-existence of a small amount of tellurium seems to improve deoxidation of steel with aluminum.The practical realization requires a subsequent treatment upon which the residual tellurium must be removed out of steel. The three experimental examinations led to the following conclusions:
1) Ar stream can fast rid molten iron of tellurium. 40%-50% of tellurium was taken away for 20 min. under the present experimental conditions. The rate satisfies the general kinetic equation for vaporization of alloying elements.
2) Rare earth metal is the most suitable substance to be added for the present aim, i. e. the removal of tellurium at low oxygen potential.
3) A flux of CaF₂-CaCN₂ mixture is applicable instead of expensive REM. The mixture with a composition ratio of 1:1 succeeded in reducing the residual concentration of tellurium to about 20 ppm (rd. 90% reduction of tellurium) during 20 min. treatment with little change in the concentrations of oxygen, carbon and nitrogen in the melt.

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Equilibria between Mn Alloy Melts Satulated with C and Various Kinds of Molten Slags and Calculation of the Activities

Akihiko TANAKA

pp. 1474-1483

抄録

In order to make clear the physical chemistry of the distribution reaction of Mn and Si between alloy melts and molten slags in the production furnace of high carbon ferromanganese and silicomanganese, the Mn-Si-C_sat. and Mn-Fe-Si-C_sat. alloy melts were equilibrated with MnO-SiO₂, CaO-MnO-SiO₂, CaO-MnO-Al₂O₃-SiO₂ and CaO-MnO-Al₂O₃-MgO-SiO₂ slags. From these experimental results, following thermochemical values were calculated by using the activities obtained previously by the author and some investigators;
(1) The activities of Si in Mn-Si-C_sat. melts at 1500 and 1550°C, and in Mn-Fe-Si-C_sat. melts at 1500°C.
(2) The activities of SiO₂ in CaO-MnO-SiO₂ molten slags at 1500°C.
(3) The values of a_MnO²/a_SiO₂ in CaO-MnO-Al₂O₃-SiO₂ molten slags at 1500°C.
(4) The values of a_MnO²/a_SiO₂ in CaO-MnO-Al₂O₃-MgO-SiO₂ molten slags equilibrated with Mn-Fe-Si-C_sat. alloy melts at 1600°C.

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雑録

鉄と鋼 Vol.41(1955), No.4

Manganese Ores used for Production of High Carbon Ferromanganese

鉄と鋼 Vol.49(1963), No.7

Oxidation-Reduction Equilibria of Manganese in Mn_tO-CaO-SiO₂-Al₂O₃ Melts

鉄と鋼 Vol.73(1987), No.16

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Thermodynamics of Fe_tO-M_xO_y (M_xO_y= CaO, SiO₂, TiO₂, and Al₂O₃) Binary Melts in equilibrium with Solid Iron

Shiro BAN-YA, Akira CHIBA, Akihide HIKOSAKA

pp. 1484-1493

抄録

As a fundamental study of physical chemistry of steelmaking slags, equilibria between hydrogen-water gas mixture and liquid slags contained in solid iron crucibles have been measured for four binary slags of Fe_tO-CaO, Fe_tO-SiO₂, Fe_tO-TiO₂ and Fe_tO-Al₂O₃ systems at 1400 °C. From the data, the activity of iron oxide and the ratio of ferrous and ferric iron (Λ = Fe³⁺/Fe²⁺) were calculated for the composition of slags. In view of ionic theory, a regular solution model for cations was applied to evaluate the thermodynamic properties of complex slags from those of the binary slags. Three binary slags of Fe_tO-SiO₂, Fe_tO-CaO and Fe_tO-TiO₂ systems conformed to the regular solution model within the experimental error except for the extremely FeO rich region. It was confirmed that the oxygen distribution between slag and metal was quantitatively expressed with this model over the wide range of slag composition.

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The Thermodynamics of Titanium in Molten Slags Equilibrated with Graphite

鉄と鋼 Vol.67(1981), No.14

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Rate of Hydrogen Desorption from Liquid Iron Alloys

Shiro BAN-YA, Kenzo MORI, Yukio TANABE

pp. 1494-1501

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The rates of hydrogen desorption from liquid iron and several liquid binary iron alloys were measured by the carrier gas method using argon. The results obtained are summarized as follows.
1. The rate of hydrogen desorption from liquid iron is governed by a first order reaction for hydrogen content in iron.
2. The rate of reaction is largely affected by the agitation of liquid iron.
3. The activation energy of the reaction obtained is a fairly low value of 5.7 kcal/mol.
4. From the facts mentioned above, the rate of hydrogen desorption from liquid iron is controlled by the transport of hydrogen atoms in the boundary layer of the liquid phase, and the value of mass transfer coefficient in the inductively stirred melt is 3.16 × 10^-2 cm/sec for pure iron at 1600 °C.
5. As the effect of alloying elements, the reaction rate decreases with carbon and chromium contents, and increases with silicon content. Nickel has no measurable effect.
6. A good correlation was found between the present values of mass transfer coefficients of hydrogen in the alloy systems and the diffusion coefficients of hydrogen in iron alloys reported by H. Bester and K. W. Lange.

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Model Experiment and Theoretical Analysis on Structure of Inverse V-segregation

Shigeo ASAI, Hajime INOUE, Hakaru NAKATO, Iwao MUCHI

pp. 1502-1511

抄録

Concerning the formation of macrosegregation in ingots, it is well known that the channels are smooth on the side facing outside of ingot and rough facing inside of ingot.
In this work, these phenomena were reproduced by a model experiment of NH₄Cl-H₂O system and the progress of channel formation was precisely visualized. The experiment indicated that the channels were melted on the side facing outside of ingot and solidified on the other side, and that the interdendritic liquid flowed into the channels through the wall facing inside of ingot and a part of the liquid flowed out the channels through the other wall. The difference in the roughness between the both walls is theoretically explained on the basis of transport phenomena in this paper.

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Study on the Descaling of the Steel Slabs before Hot Rolling

Toshiro FUKUTSUKA, Takayuki NAKAMURA, Moto SATO, Ichiro KOKUBO, Ryuichi ISHIDA

pp. 1512-1521

抄録

The factors affecting on the descaling property of reheated steel slabs have been studied in the plate rolling shop. The frequency of scale defects is closely related to the amount of residual scale on the steel slabs after descaling by the hydraulic scale breaker. It is found in the rolling shop that the amount of the residual scale depends remarkably on the following two factors.
(1) Degree of overheating in the furnace
(2) Surface temperature of the scale on slabs immediately before descaling.
On the other hand, it has been pointed out by many workers that the descaling property of Si-killed steels are worse than semi-killed steels. It is well known that fayalite is formed in the scale of Si-killed steel. In this study the effect of surface temperature of scale on the descaling property is mainly examined. It is found experimentally that the existence of fayalite causes the cracks in the scale during cooling.
It could be concluded that the descaling property tends to be bad for the Si-killed steels when the cracks are formed in the scale before descaling.

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Effect of Intercritical Rolling by Hot Strip Mill on the Strength and Notch Toughness of Plain Carbon Steel

Susumu GOHDA, Kunio WATANABE, Yoshio HASHIMOTO, Hideo HIRAYAMA, Satoshi KIJIMA

pp. 1522-1531

抄録

The application of the intercritical rolling on plain carbon steel, of which beneficial effect on strength and notch toughness was proved by laboratory mill experiment, has been made to hot strip mill.
The following results are obtained:
(1) Both spiral-welded and electric-resistance-welded pipes manufactured of intercritically-rolled coils show strength of X 52 grade and good notch toughness at low temperature.
(2) Improvement of strength and notch toughness in intercritically-rolled coils are due to grain refinement of ferrite and pearlite which are transformed from worked austenite, and formation of substructure in ferrite worked in intercritical range.
(3) No disadvantageous influence of intercritical rolling is observed such as lowering of strength or deterioration of notch toughness in welds in comparison to conventionally-rolled steel.
(4) Though the intercritically-rolled coils have the texture in midthickness similar with that of cold rolled plate with strong fiber structure having<110>-axis parallel to rolling direction as main component, the mechanical properties as pipes are good as the change of properties due to pipe manufacturing is small and anisotropy of yield strength even decreases.
It is concluded that the intercritically-rolled strip is suitable for structural steel required high yield strength and good notch toughness such as high-test line pipe.

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Development of Low Carbon Equivalent and Normalized HT50 Steel with High N-V Addition

鉄と鋼 Vol.77(1991), No.1

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A New Tempering Parameter and Its Application to the Integration of Tempering Effect of Continuous Heat Cycle

Tsuyoshi INOUE

pp. 1532-1541

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A new tempering parameter (λ-value) has been defined basing on Arrhenius' equation so as to express the degree of tempering and to maintain the equivalence of time and temperature over a wide range of tempering conditions.
Activation energy of the tempering process governing the changes in such mechanical properities as tensile and yield strength and hardness was determined by using a plain carbon steel and low alloy steels containing manganese, chromium and molybdenum. The activation energies obtained were to be 70 kcal/mol (295 kJ/mol) in carbon steel and about 100 kcal/mol (420 kJ/mol) in Cr-Mo steel, increasing with alloy contents.
Using these activation energies, mechanical properties of tempered steel can be approximately expressed as a function of λ-value in a linear fashion for any combination of temperature and time, ranging from 400 °C to 700 °C and from 0.01 h to 1000 h, respectively.
In addition, making use of the parameter, an analytical method of tempering effect is applied to a practical heat program by summarization of the tempering effects of two individual processes or integration of the tempering effect over a whole process of heat cylce in which temperature steadily changes. Predicted mechanical properties by this method were in good accordance with observed values.

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Effect of Specimen Shape on the Delayed Failure Strength of High Strength Steel Prestressed by Partial Unloading

Keijiro NAKASA, Mitsuo KIDO, Hideo TAKEI

pp. 1542-1549

抄録

The effects of two types of prestressing, i.e. partial unloading and perfect unloading, on the delayed failure strength have been investigated on various specimen configurations.
The results obtained are summarized as follows:
(1) Crack initiation time and 100 h delayed failure strength can be largely increased by two types o prestress methods, especially by partial unloading method, regardless of specimen thickness and notch root radius. The rate of increase of 100 h delayed failure strength by both prestress methods increases to converge to a certain value with increase of specimen thickness.
(2) In order to raise the 100 h delayed failure strength by both prestressing methods, it is necessary to increase the unloading stress to a critical value, (σ_a)_c, which increases with increase of specimen thickness and decrease of notch root radius.

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Measurement of Apparent Viscosity of Ferrous and Non-ferrous Alloys in Liquid/solid Coexisting State-Fe-C, Sn-Pb, Al-Cu and Fe-Cr-Ni-C Alloys

Akihiko SHIBUTANI, Kazuhiko ARIHARA, Yasushi NAKAMURA

pp. 1550-1556

抄録

Measurement was made on viscosities of partially solidified binary alloys Fe-C (3 and 4%C), Sn-Pb (1.0, 1.5, 5, 15, 25, and 45%Pb), and Al-Cu (4.5 and 10%Cu), and iron-base alloys (Fe-2%Cr-1.5%C, Fe-25%Cr-20%Ni-0.4%C, and Fe-28%Cr-0.4%C). A rotating coaxial cylinder viscometer was used. Solid fraction was calculated for the observed temperatures with the aid of the equation proposed by Scheil. The viscosities were found to depend on the solid fraction, the cooling rate, and the shear rate, as has been reported by FLEMINGS.
When the calculated value of solid fraction was more than 0.6 at the eutectic temperature, the relation between the viscosity and the solid fraction was similar to that for dispersed systems; that is, the viscosity increased remarkably in the range of solid fraction over about 0.5. When the calculated solid fraction at the eutectic temperature was less than 0.6, the viscosity rapidly increased after the temperature of alloy reached the eutectic one.
The viscosity of the iron-base alloys was found to be affected more intensively by the cooling rate than by the shear rate.

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Materials Problem in Coal Gasification and Liquefaction Processes

Yoshinao MISHIMA

pp. 1557-1564

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Recent Research Development of Amorphous Alloys in the U. S. A.

Shinji TAKAYAMA

pp. 1565-1568

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良い英文を書くために/一カナダ人の見た1980年春季講演大会

Roderick I. L. GUTHRIE

pp. 1569-1575

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黒田浩一, 雀部実, 小松周作, 月橋文孝, 新谷一憲, 小林一彦, 虎岩清, 檀武弘, 郡司好喜, 大沼啓明, 望月俊男, 斎藤鉄哉, 青木孝夫, 村上雅人, 長井寿, 名村夏樹, 篠崎正利

pp. 1581-1587

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21 Dec. (Last 30 Days)

Wettability of CaS against molten iron at 1873 K

ISIJ International 早期公開
凝固過程における溶鋼中からAl₂O₃上へのMnSの晶出挙動

鉄と鋼早期公開
Reduction and Melting Behaviors of Iron Oxide Composite with Carbon Deposited Using CO-CO₂-H₂ Mixed Gas

ISIJ International 早期公開
In-situ Observation of Precipitation and Growth of MnS Inclusions during Solidification of a High Sulfur Steel

ISIJ International Vol.64(2024), No.14
Perspectives on the Promising Pathways to Zero Carbon Emissions in the Steel Industry toward 2050

ISIJ International 早期公開
モデル材料を用いた凝固過程における介在物生成挙動のその場観察

鉄と鋼早期公開
Transition behavior of gas containing suspension from solid-like to liquid-like flows

ISIJ International 早期公開
A hot rolling full process rolling force prediction method based on transfer learning and Inception-LSTM neural network

ISIJ International 早期公開
Slag-steel reactions in the refining of Advanced High-Strength Steel

ISIJ International 早期公開
Chemical and Mechanical Factors on Phosphorus Dissolution Behavior from P-concentrated Slag

ISIJ International Vol.64(2024), No.14

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鉄と鋼 Vol. 66 (1980), No. 10

キーワードランキング

hydrogen reduction of iron ore

gasification

characterization of coal and biomass based on kinetic parameter distributions for pyrolysis

kinetics of decarburization of liquid iron with high concentration ofcarbon

mechanisms of liquefaction and pyrolysis reaction of biomass

hydrogen reduction

steel

19al6mg

automotive wheel

deguchi

鉄と鋼 Vol. 66 (1980), No. 10

Oxidation of Sulfur in B. F. Slags to Sulfate

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Removal of Tellurium out of Molten Iron

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Equilibria between Mn Alloy Melts Satulated with C and Various Kinds of Molten Slags and Calculation of the Activities

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Thermodynamics of FetO-MxOy (MxOy= CaO, SiO2, TiO2, and Al2O3) Binary Melts in equilibrium with Solid Iron

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Rate of Hydrogen Desorption from Liquid Iron Alloys

SNSによる共有

Model Experiment and Theoretical Analysis on Structure of Inverse V-segregation

SNSによる共有

Study on the Descaling of the Steel Slabs before Hot Rolling

SNSによる共有

Effect of Intercritical Rolling by Hot Strip Mill on the Strength and Notch Toughness of Plain Carbon Steel

SNSによる共有

A New Tempering Parameter and Its Application to the Integration of Tempering Effect of Continuous Heat Cycle

SNSによる共有

Effect of Specimen Shape on the Delayed Failure Strength of High Strength Steel Prestressed by Partial Unloading

SNSによる共有

Measurement of Apparent Viscosity of Ferrous and Non-ferrous Alloys in Liquid/solid Coexisting State-Fe-C, Sn-Pb, Al-Cu and Fe-Cr-Ni-C Alloys

SNSによる共有

Materials Problem in Coal Gasification and Liquefaction Processes

SNSによる共有

Recent Research Development of Amorphous Alloys in the U. S. A.

SNSによる共有

良い英文を書くために/一カナダ人の見た1980年春季講演大会

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抄録

SNSによる共有

論文アクセスランキング

Wettability of CaS against molten iron at 1873 K

凝固過程における溶鋼中からAl2O3上へのMnSの晶出挙動

Reduction and Melting Behaviors of Iron Oxide Composite with Carbon Deposited Using CO-CO2-H2 Mixed Gas

In-situ Observation of Precipitation and Growth of MnS Inclusions during Solidification of a High Sulfur Steel

Perspectives on the Promising Pathways to Zero Carbon Emissions in the Steel Industry toward 2050

モデル材料を用いた凝固過程における介在物生成挙動のその場観察

Transition behavior of gas containing suspension from solid-like to liquid-like flows

A hot rolling full process rolling force prediction method based on transfer learning and Inception-LSTM neural network

Slag-steel reactions in the refining of Advanced High-Strength Steel

Chemical and Mechanical Factors on Phosphorus Dissolution Behavior from P-concentrated Slag

詳細検索

Thermodynamics of Fe_tO-M_xO_y (M_xO_y= CaO, SiO₂, TiO₂, and Al₂O₃) Binary Melts in equilibrium with Solid Iron

凝固過程における溶鋼中からAl₂O₃上へのMnSの晶出挙動

Reduction and Melting Behaviors of Iron Oxide Composite with Carbon Deposited Using CO-CO₂-H₂ Mixed Gas